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Synthesis was done via distillation since it helps in obtaining purer substances (Bernard-Chandler, n,d). Gas chromatography-Mass Spectroscopy is a physical method of separating a compound which are volatile and thermally stable.Learn More
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The Williamson synthesis cannot be used with tertiary alkyl halides because they undergo elimination reactions instead of participating in S N 2 reactions. Thus, to make an unsymmetrical ether with a primary and a tertiary alkyl group, a primary alkyl halide and a tertiary alkoxide ion are the best reagents. For example, tert-butyl methyl ether can be prepared by the reaction of sodium tert.Learn More
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